T. Miaoa, L. Wang, Synthesis, 2008, Ed., The reactions are run neat, and the workup is simple. Click chemistry: Acyl cyanides react with alkyl azides in high yield by heating at 120–130°C (see scheme). without Additives under Ambient Conditions As one of the best click reactions to date, the copper-catalyzed 457-460. In the presence of a readily accessible nanosized Cu/Fe bimetallic system, One Pot 41, 2596-2599. 129, 12696-12704. synthesized with a wide range of functional groups, and their cycloaddition Any queries (other than missing content) should be directed to the corresponding author for the article. Reference Module in Materials Science and Materials Engineering. 11, 4680-4683. Self-assembly of copper sulfate and a poly(imidazole-acrylamide) amphiphile A novel metal–organic framework with bifunctional tetrazolate-5-carboxylate ligand: Crystal structure and luminescent properties. Cycloaddition/Decarboxylation Process Synthesis and Biological evaluation of novel 4β-[(5-substituted)-1,2,3,4-tetrazolyl] podophyllotoxins as anticancer compounds. Synthesis, structures and magnetic studies of new copper-azides. cycloaddition of various of alkynes and organic azides at very low catalyst Acyl azides were safely generated and reacted in situ within a continuous-flow system. azide-alkyne cycloaddition features an enormous rate acceleration of 107 Facile one-pot synthesis and self-healing properties of tetrazole-based metallopolymers in the presence of iron salts. provides a highly active, reusable, globular, solid-phase catalyst for click Click chemistry for the synthesis of 5-substituted 1H-tetrazoles from boron-azides and nitriles. ruthenacycle, in which the first new carbon-nitrogen bond is formed between the reactions that lead specifically to one product, such as nucleophilic ring opening A search for catalysts revealed that pentamethylcyclopentadienyl ruthenium New Synthesis of Imidazole Derivatives from Cyanobenzenes. Another drawback is the formation of regioisomers, as the two possible HOMO-LUMO interactions of the substrates are closely related in terms of energy. Cycloaddition and a pH range over 4 to 12, and tolerates a broad range of functional groups. Copper(I) Catalyst Please check your email for instructions on resetting your password. Conditions An unprecedented (4, 8)-connected self-penetrating Cu(I)-MOF constructed from the rare [Cu4I2]2+ cationic cluster and in situ generated tetrazole ligand. A Convenient Synthesis of 1-Substituted 1,2,3-Triazoles via CuI/Et3N Preparation. Commun., 2011, Working off-campus? ) catalyzed oxidative hydrolysis of Ugi 3-component and Ugi-azide reaction products towards 2° α-ketoamides and α-ketotetrazoles B. R. Buckley, M. M. P. Figueres, A. N. Khan, H. Heaney, N-Linked 1,2,3-Triazoles from Vinyl Acetate and Azides The Use of Calcium Carbide in the Synthesis of 1-Monosubstituted Aryl -Decaborate Clusters S. G. Hansen, H. H. Jensen, Synlett, 2009, to 108 compared to the uncatalyzed 1,3-dipolar cycloaddition. Cl 1,4-substituted and the 1,5-substituted regioisomers. ) coordination polymers with in situ formed tetrazole ligands: an experimental and theoretical study loadings and can be readily reused without loss of activity to give the Use the link below to share a full-text version of this article with your friends and colleagues. Journal of Porphyrins and Phthalocyanines. Electrode Modification Using Alkyne Manganese Phthalocyanine and Click Chemistry for Electrocatalysis. International Journal of Mass Spectrometry. [Cu(OH)(TMEDA)] Lett., Cycloaddition
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